Structural Study and Chemical Composition Analysis ‎of the Historical Adobe from the Surviving ‎Architectural Structures in the Borj-e Afghan Region ‎of Sistan - Journal of Research on Archaeometry
------------------------------------------ ---------------------------------------
year 11, Issue 2 (2025)                   JRA 2025, 11(2): 0-0 | Back to browse issues page


XML Persian Abstract Print


Download citation:
BibTeX | RIS | EndNote | Medlars | ProCite | Reference Manager | RefWorks
Send citation to:

Bater M, Rostampour M. (2025). Structural Study and Chemical Composition Analysis ‎of the Historical Adobe from the Surviving ‎Architectural Structures in the Borj-e Afghan Region ‎of Sistan. JRA. 11(2), : 7 doi:10.66224/jra.2025.11.207
URL: http://jra-tabriziau.ir/article-1-488-en.html
1- Faculty of Art, University of Birjand, Birjand, Iran , masoud.bater@birjand.ac.ir
2- Conservation & Restoration of Cultural Properties, University of Zabol, Zabol, ‎Iran
Abstract:   (975 Views)
Mudbrick and earthen architecture in the Middle East, particularly in Iran, has a long-standing ‎tradition ‎and remarkable continuity due to the arid climate and the abundance of soil ‎sediments. Archaeological ‎evidence from eastern and southeastern Iran, including the Sistan ‎region and sites such as Shahr-e ‎Sukhteh, Dahaneh-ye Gholaman, and Old Zahedan ‎‎(Zahedan-e Kohneh), demonstrates the persistence ‎of this technology from prehistoric times ‎through the Islamic periods. Despite this extensive ‎background, detailed laboratory studies ‎on the materials of historical mudbrick and earthen buildings in ‎this region remain ‎limited.The aim of this research is to identify the structure and determine the chemical ‎composition of historical ‎mudbricks from the Islamic period in the rabad area of Zahedan-e ‎Kohneh‎, in order to provide a ‎scientific basis for assessing material conditions and ‎supporting conservation and restoration decision-‎making for earthen architecture. To this ‎end, a set of historical mudbrick samples from the Afghan ‎Tower area was examined using ‎standard laboratory techniques, including X-ray fluorescence (XRF), X-‎ray diffraction (XRD), ‎titration analysis, and gravimetric determination of sulfate content.‎The results indicate that ‎the mudbricks were produced from local, alluvial, and heterogeneous soils with ‎a clay–‎siliceous composition containing carbonate and gypsum lenses. The presence of mineral ‎phases ‎such as quartz, feldspars, calcite, dolomite, muscovite, and montmorillonite, together ‎with a wide ‎dispersion of calcium carbonate (9–40.5%) and calcium sulfate (0.26–1.4%), ‎reflects the heterogeneity of ‎the original material composition and the potential reactivity of ‎the materials in response to moisture ‎and salt-related factors.‎The findings underscore the ‎necessity of considering conservation constraints and conducting ‎supplementary ‎investigations and tests prior to any consolidation interventions. By providing chemical ‎and ‎mineralogical data, this study establishes a preliminary framework for the scientific support of ‎‎conservation and restoration decision-making for earthen buildings in the region and ‎highlights the ‎critical role of material composition analysis in evaluating their stability ‎conditions.‎
Article number: 7
Full-Text [PDF 1842 kb]   (136 Downloads)    
Technical Note: Original Research | Subject: Archaeometry
Received: 2025/09/27 | Accepted: 2025/12/29 | Published: 2025/12/30 | ePublished: 2025/12/30

References
1. Alavéz-Ramírez., R, Montes-García, P., Martínez-Reyes, J., Altami-rano-Juárez, D. C., & Gochi-Ponce, Y. ‎‎(2012). The use of sugarcane bagasse ash and lime to improve the durability and mechanical properties ‎of compacted soil blocks. Construction and Building Materials, 34, 296-305.‎ [DOI:10.1016/j.conbuildmat.2012.02.072]
2. Ascensao, G., Pereira, J., Fonseca, J., Costa, A., Ferreira, V. M., & Paiva, H. (2025). Reviving heritage with contemporary solutions for adobe wall rehabilitation. Construction and Building Materials, 458, 139557. [DOI:10.1016/j.conbuildmat.2024.139557]
3. Bater M, Serajii ‎ F. (2022). Studies on the Body Structure of the Islaim Period Slip-painted Pottery Shards of Sistan. Journal of Research on Archaeometry. 8(2), 47-64. [in Persian]
4. Bater, M. and Serajii, F. (2023). Identification of the Chemical Com-position of the Slip Coating and the Colors Used in Some Slip-painted Pottery ‎from the Sistan Region. Journal of Studies in Color World, 13(3), 269-282. [in Persian]
5. Bater M, Ahmadi H, Abedi Koupai J, Emadi R. The Effect of Curing Time on Compressive and Tensile Strength of Traditional Kahgel. Journal of Housing and Rural Environment. 2017 Jun 10;36(157):69-86. [in Persian]
6. Behboodi, N., & Zohreh, . (2020). Investigating the Architectural Ad-aptation of the Kharkhaneh Chamber of Machi Castle (Safavid Period) ... Iranian Archaeological Research Journal, 10(24), 187-205.
7. Calatan, Gabriela, G., Hegyi, A., Dico, C., & Mircea, C. (2016). De-termining the Optimum Addition of ‎Vegetable Materials in Adobe Bricks. Procedia Technology, 22, 259-265.‎ [DOI:10.1016/j.protcy.2016.01.077]
8. Corrêa, Andréa Aparecida Ribeiro, Lourival Marin Mendes, Normando Perazzo Barbosa, Thiago de Paula ‎Protásio, Nathalia de Aguiar Campos, ‎&‎ Gustavo Henrique Denzin Tonoli. (2015). Incorpora-tion of ‎bamboo particles and "synthetic termite saliva" in adobes. Construction and Building Materials, 98, 250-‎‎256.‎ [DOI:10.1016/j.conbuildmat.2015.06.009]
9. Charola, A. E. (2000). Salts in the deterioration of porous materials: An overview. Journal of the American Institute for Conservation, 39(3), 327-343. [DOI:10.1179/019713600806113176]
10. Charola, A. E., Pühringer, J., & Steiger, M. (2007). Gypsum: A review of its role in the deterioration of building materials. Environmental Gology, 52(2), 339-352 [DOI:10.1007/s00254-006-0566-9]
11. Davtalab, J. (2021). A Study of the Architecture and Urban … (Daha-neh-e Gholaman). Journal of Sistan and Baluchistan Studies.
12. Demay, L., Péan, S., & Patou-Mathis, M. (2012). "Mammoths used as food and building resources by ‎Neanderthals: Zooarchaeological study applied to layer 4, Molodova I (Ukraine)", Quaternary In-ternational, 276, ‎‎212-226. [DOI:10.1016/j.quaint.2011.11.019]
13. Doat, P., Hays, A., Houben, H., Matuk, S., & Vitoux, F. (1990). Con-struire en terre. Paris: Éditions Alternatives
14. ‎Eftekhari, N., Holakooei, P., Sayyadshahri, H., & Vaccaro, C. (2018). Four shades of black: Non-invasive scientific studies on the painted potteries from Shahr-i Sokhta, eastern Iran. Journal of Archaeo-logical Science: Reports, 22, 100-107. [DOI:10.1016/j.jasrep.2018.09.012]
15. Eires, R., Aires Camões, & Said Jalali (2013). Earth architecture: ancient and new methods for durability ‎improvement. ICSA2013-2nd In-ternational Conference on Structures and Architecture. CRC Press Taylor ‎& Francis Group, 962-970.
16. El-Mahllawy, Medhat S., and Ayman M. Kandeel. (2014). Engineering and mineralogical characteristics of ‎stabilized unfired montmoril-lonitic clay bricks. HBRC Journal, 10‎‏)‏‎1‎‏(‏‎, 82-91.‎ [DOI:10.1016/j.hbrcj.2013.08.009]
17. Farnow, B. (2005). The origins of culture, civilization, and art in ancient Mesopotamia (1st ed.). Sureh ‎Mehr, Tehran. [in Persian]
18. Gardner, H. (2008). Art through the ages (M. T. Foramarzi, Trans.; 9th ed.). Agah va Negah, Tehran‎. [in Persian]
19. Hejazi M, Hashemi M, Jamalinia E, Batavani M. (2015). Effect of Ad-ditives on Mechanical Strengths of ‎Adobe Made From Soils of Is-fahan. Journal of Housing and Rural Environment, 34 (151), 67-80‎
20. ‎Houben, Hugo; Guillaud, Hubert. (1994). Earth Construction: A Comprehensive Guide, Intermediate technology Publications, London.
21. Ghanimati, S. (2000). New Perspectives on the Chronological and Functional Horizons of Kuh-e Khwaja in Sistan. Iran, 38, 137-150 [DOI:10.2307/4300589]
22. Goudie, A. S., & Viles, H. A. (1997). Salt weathering hazards. Chichester: John Wiley & Sons. [DOI:10.1007/978-94-011-5228-0_6]
23. Hall, M., & Djerbib, Y. (2004). Rammed earth construction. London: BRE Press.
24. Hadian Dekordi. M (2016). Soil studies of historical and ancient mud-brick materials in various regions of ‎Iran. Athar Quarterly, 37(75), 85-96. in Persian]
25. Hajirasouliha B, Kiani-DehKiani G, Heidari D, Emami M. (2024). Analysis of the Effect of Soil Properties on the Mechanical Re-sistance of Historical Mud-Bricks of Yazd. Journal of Research on Archaeometry. 10(1), 145-166.
26. Heathcote, K. (2011). Durability of earthwall buildings. London: Routledge.
27. Houben, H., & Guillaud, H. (1994). Earth construction: A comprehen-sive guide. London: Intermediate Technology Publications. [DOI:10.3362/9781780444826]
28. Majidzadeh, Y. (1997). History and civilization of Mesopotamia, Volume 1: Political history. Markaz-e ‎Nashr-e Daneshgahi, Tehran. [in Per-sian]
29. Masoumi, G. R. (2004). History of archaeology. Samt, Tehran‎. [in Per-sian]
30. Malek Shahmirzadi, S. (2011). Mesopotamia in prehistory. Sohban Noor va Ganjineh-ye Naqsh-e ‎Jahan, Tehran. [in Persian]
31. Mousavi Haji, S. R. (2009). Zahedan-e kohne the abandoned city in sistan‎. Paazh Publishing, Mashhad‎.[in Persian]
32. Mousavi haji. S.R, Mehrafarin. R. and Alaei Moghadam, J. Review the Environmental Characteristics of Historical City of Zahedan-e-Kohne. J Geography and Development. 2011: 79-96. [in Persian]
33. Minke, G. (2012). Building with earth: Design and technology of a sustainable architecture. Basel: Birkhäuser. [DOI:10.1515/9783034608725]
34. Miri, N. K., Sarhaddi-Dadian, H., Bahramzadeh, K., & Hashemi-Baghi, M. (2020). Comparison of vulnerability conditions of adobes' structure-the study of historical and restored adobes of Kooh-e Khajeh ancient site (Kohan Dezh castle) in Sistan, Iran. Iran, Ma-teriale și Cercetări Arheologice, 15, 267-278. [DOI:10.3406/mcarh.2020.2140]
35. Miqueleiz, L; Ramirez, F; Oti, J.E; Seco, A; Kinuthia, J.M; Oreja, I & Urmeneta, P. (2013). Alumina filler ‎waste as clay replacement material for unfired brick production. Engineering Geology, 163, 68-74.‎ [DOI:10.1016/j.enggeo.2013.05.006]
36. Moradi, H. (2020). Architectural Style and Technique in Prehistoric Sistan: Sustainable Patterns in Shahr-i Sokhta Architecture from Early 3rd Millennium to the Beginning of the 2nd Millennium BC. Ash-Sharq: Bulletin of the Ancient Near East - Archaeological, Historical and Societal Studies, 4, 57-89.
37. Mousavi Haji, S. R. (2009). Zahedan-e Kohne: The abandoned city in Sistan [Book in Persian]. Mashhad, Iran: Paazh Publications.
38. Nwankwor, N. A. (2011). Justification for the Combination of Organic and Inorganic Stabilizers to ‎Stabilize Traditional Earth Materials (Mud) for Quality and Capacity Utilization in Africa. In Terra 2008: ‎The 10th International Conference on the Study and Conservation of Earthen Architectural Heritage, ‎Getty Publications, 239-246.‎
39. Parchebaf motlagh, F. , Alemi, B. and sadeghpour, A. H. (2024). The study of the Characteristics of Clay in Four Historical Monuments in Kashan. Soffeh, 34(4), 107-137. doi: 10.48308/soffeh.2024.105153. [in Persian]
40. ‎Perrot, J., Le Brun, A., & Labrousse, A. (1971). "Recherches ar-chéologiques à Suse et en Susiane en 1969 et en ‎‎1970", Syria 48, 21-51.‎ [DOI:10.3406/syria.1971.6232]
41. ‎Perrot, J. (1981). "L'architecture militaire et palatiale des Achéménides à Suse", in 150 Jahre Deutsches ‎Archäologisches Institut 1829-1979, Internationales Kolloquium, and Mainz: Neue Ergebnisse archäologischer ‎Stadtforschung, 79-94.
42. Pedram B, Ebrahimi A. (2017). Structural and Physical Characteristics of the Adobe Bricks Used at the World Heritage Site of Arg-e Bam. Journal of Research on Archaeometry. 3(2), 81-102. [in Persian] [DOI:10.29252/jra.3.2.81]
43. Rahimnia, R & Heidari Bani, D. (2011). The Effect of Plasticity Index (PI) on the Tensile and Compressive ‎Strength of Cement-Stabilized Adobes for Conservation of Adobe Structures. Journal of conser-vation ‎studies and cultural sites research, 1 (2), 91-102.‎
44. Sharma, Vandna, Hemant K. Vinayak, and Bhanu M. Marwaha (2015). Enhancing sustainability of rural ‎adobe houses of hills by addition of vernacular fiber reinforcement. International Journal of Sustainable ‎Built Environment, 4(2), 348-358.‎ [DOI:10.1016/j.ijsbe.2015.07.002]
45. ‎‎Stronach, D., Roaf, M., & London British Institute of Persian Studies. (2007). Nush-i Jan. 1. The major ‎buildings of the Median settlement. Peeters, London.
46. Tate, G. P. (1977). Seistan: A memoir on the history, topography, ruins, and people of the country.
47. Torraca, G. (2009). Lectures on materials science for architectural con-servation. Los Angeles: Getty Conservation Institute.
48. Tohidi M. (2004). Argnameh: Aperspective on the Bam Citadel in the historical context. Kerman Studies Center. [in Persian]
49. [in Persian]
50. Walker, P. (1979). Strength and erosion characteristics of earth blocks and earth block masonry. Oxford: Oxford Polytechnic.
51. Wons, W., Kłosek-Wawrzyn, E., & Rzepa, K. (2025). Corrosion of porous building ceramics caused by double sulphate salt. Materials, 18(5), Article 1041 [DOI:10.3390/ma18051041]
52. Zhang, J; Chen, W; Li, Z; Wang, X; Guo, Q & Wang, N. (2015). Study on workability and durability of calcined ‎ginger nuts-based grouts used in anchoring conservation of earthen sites. Journal of Cultural Heritage, ‎‎16, 831-837‎. [DOI:10.1016/j.culher.2015.02.007]
53. Zakavi S, Ebrahimi A. (2023). Provenance studies of the clay used in mudbricks from Chogha- Zanbil, Elmite period, on optimization ofmudbricks applied in conservation. Journal of Research on Archaeometry. 9(2), 173-191. [in Persian]

Rights and permissions
Creative Commons License This work is licensed under a Creative Commons Attribution-NonCommercial 4.0 International License.

© 2026 CC BY-NC 4.0 | Journal of Research on Archaeometry

Designed & Developed by : Yektaweb