Preparation of Thin Sections of Porous Materials for Polarizing Microscope Investigation in Archaeometry - Journal of Research on Archaeometry
year 3, Issue 2 (2017)                   JRA 2017, 3(2): 45-60 | Back to browse issues page


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Razani M, Martinez Conejero F, Mansori Isfahani M, Afsharinezhad H. Preparation of Thin Sections of Porous Materials for Polarizing Microscope Investigation in Archaeometry. JRA. 2017; 3 (2) :45-60
URL: http://jra-tabriziau.ir/article-1-34-en.html
1- Assistant Professor Tabriz Islamic Art University , m.razani@tabriziau.ac.ir
2- Lecturer Department of Geosciences and Environment, University of Alicante
3- Assistant Professor, Faculty of Mining Engineering, Dep. Mine Engineering, Industrial University of Isfahan Isfahan University of Technology
4- M.Sc. in Archaeometry Tabriz Islamic Art University
Abstract:   (578 Views)
Thin section petrography is a knowledge based on a study of stones and minerals with polarizing light of a transmitting optical microscope, that is a standard scientific method for mineralogy, petrology, geology and etc. Researchers with this method can gain supplementary or fundamental information. Thin section making technique was developed by geologists for the study of rocks. Using the thin section for the study of cultural heritage has more than one century old. Thin sections take into consideration from a basic analysis for use to examine a wide variety of Archaeometry-archaeological survey and also conservation and of historical materials for characterization, determining sources and provenance, pathology and evaluation of the conservation treatment effect on inorganic materials (such as: rocks, historical slags, mud brick, plaster, pottery and ancient mortars).Thin sections use for petrological and mineralogical survey are made in different sizes by using different techniques for curing, polishing and staining small slabs of a rock sample,normally thin sections made by reducing the thickness of small fragments of materials that attaching the flat surface of glass microscope slide (with size of 47×26 mm) by sawing and grinding to standardthickness (25-30µm),at this thickness most mineral s (e.g. silicatestypically quartz is used as the reference to determine standard thickness as it is one of the most abundant minerals) becomes more or less transparent and can then be observed by a microscope using transmitted light and then using the Michel-Lévy interference color chart to recognizing the minerals and their structural aspects (cleavage, fractures, mineral zoning).On one hand when the ordinary methods of making thin sections applied to other materials that are soft, heat sensitive, and/or water sensitive, thin section preparation presents considerable challenges for the technician and On the other hand, according to the limitation of sampling in the case of the cultural heritage of artworks and historical objects, as we know the Archaeometry researcher most be using the minimum sample for answer the questions, Since due to the importance of saving the small and also weak samples from cultural heritage a description of preparing thin sections to Petroghraphic microscopy investigation in Archaeometry is the main purpose of this paper. Samples for this study were a kind of weak Tufa from the regions near the Alcala Del Jucar city of Valencia /Spain and also from the powdered surface of rock-hewn architecture in Kandovan Historical village from Northwest of Iran. All process for preparing the thin sections were in the petrology Lab of Geosciences and environment department from the university of Alicante/SPAIN and petrology laboratory in earth and environmental sciences department from Università degli Studi DI Milano-Bicocca, Italy. This article has been prepared in 6 essential steps, including by: 1) sampling strategy and specimen preparation, 2) preparing the samples for cutting process, 3) cutting of the fragments (consist of: hard, soft and powder materials) and making the slide, 4) impregnation techniques with a resin, and attach the slide to glass, 5) reduce the thickness of slide till standard size with sawing and grinding methods in three phase from cm to µm, and finally 6) decision making to add the protective cover for slide in the stone face plus preserve of thin section, equipments of petrography lab. the results of this study with emphasize to soft materials specialty in cultural heritage and Archaeometry demonstrated that: some steps like sampling and impregnation is very important to make high quality thin sections; consolidation and saturation of fragments with vacuum methods in two steps before any cutting can be a suitable way for materials like soft stone, weathered stone, fragile potteries and historical mortars to preparing a thin sections.
Full-Text [PDF 1309 kb]   (211 Downloads)    
Technical Note: Original Research | Subject: Archaeometry
Received: 2016/02/26 | Accepted: 2016/05/2 | Published: 2017/12/28 | ePublished: 2017/12/28

References
1. ASTM. Standard guide for petroghraphic examination of dimension stone. Stand ASTM C1721 – 09 2009.
2. ISRM. Suggested method for petrographic description of rocks, rock characterization, testing and monitoring. Int Soc Rock Mech suggest methods pergamon, Oxford 1981:75–6.
3. Reedy CL. Thin-section petrography of stone and ceramic cultural materials. Archetype; 2008.
4. Worley N. Henry Clifton Sorby (1826 1908) and the development of thin section petrography in Sheffield. Interpret silent artefacts petrol approaches to archaeological ceramics 2009:1.
5. Holmes A. Petrographic methods and calculations, 3 vols 1923.
6. Johannsen A. Manual of petrographic methods. McGraw-Hill book company, Incorporated; 1918.
7. Lepsius R. Griechische marmorstudien. Könige. Akademie der Wissenschaften.; 1890.
8. Betancourt PP, Peterson SE. Thin-section petrography of ceramic materials. Inst aegean Prehistory, archaeol excav Man 2009;2.
9. Shepard AO. Rio grande glaze paint ware: a study illustrating the place of ceramic technological analysis in archaeological research. na; 1942.
10. Felts WM. A petrographic examination of potsherds from ancient Troy. American Journal of archaeology 1942;46:237–44. [DOI:10.2307/499386]
11. Matson FR. Technological ceramic studies. Coll Art J 1942;1:25–8. doi: https://doi.org/10.2307/773399 [DOI:10.2307/773399]
12. Humphries DW. The preparation of thin sections of rocks, minerals, and ceramics 1992.
13. Quinn PS. Ceramic petrography: the interpretation of archaeological pottery & related artefacts in thin section. Archaeopress; 2013.
14. Hirsch D. How to make a thin section (Dave’s methods at WWU Geology 2012.
15. Leslie AB, Eden M. Code of practice for the petrographic examination of mortars, Plasters, Renders and Related Materials. Applied Petrography Group, UK, UK 2008:1–24.
16. Schnabel L. Geomaterials under the microscope, A colour guide: Building stone, roofing slate, aggregate, concrete, mortar, plaster, bricks, ceramics, and bituminous mixtures 2011.
17. Yaseen IAB, Al-Amoush H, Al-Farajat M, Mayyas A. Petrography and mineralogy of Roman mortars from buildings of the ancient city of Jerash, Jordan. Construction and building materials 2013;38:465–71. [DOI:10.1016/j.conbuildmat.2012.08.022]

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