After half a century, a new excavation project was launched in Orzu’iyeh (Soghan valley), south-eastern Iran where the well-published Tepe Yahya is located. Tepe Yahya was discovered in 1967 by a survey team from Harvard University under the direction of C.C. Lamberg-Karlovsky. It was occupied, with interruptions, from the late Neolithic to the early Sasanian period. Indeed, Tepe Yahya remains the main controlled excavation carried out to date within south east Iran. According to the cultural sequence of Tepe Yahya, periods VI and V appeared to be the Chalcolithic levels of the site (6th-4th Millennium BC). This paper intends to present the results of a new excavation project in this area. Due to the exciting discovery of major Bronze Age urban centers in south-eastern Iran, such as Shahr e Sukhteh (Sistan), Shahdad and Konar Sandal (Jiroft), most scholarly attention has been given to the 3rd millennium BC. As a result, the cultures preceding the Bronze Age have been often neglected, whereas the Bronze Age cultures had developed from the Chalcolithic ones. Tepe Vakilabad, as a Chalcolithic key site in the south-eastern Iran, would help us to recognize better the cultures of this era. This mound is located in the Orzu'iyeh district in the south west of Kerman province, south-eastern Iran. The area of Orzu'iyeh is known in the archeology of Iran due to the presence of Tepe Yahya and also to its strategic location. This area is a natural corridor drawn in the east-west direction connecting south of Kerman province to Fars. The eastern part of this plain includes Soghun Valley (where Tepe Yahya is situated), and the middle and western parts are respectively Dowlatabad and Vakilabad plains. This mound contains more than 4 meters of cultural layers belonging to the chalcolithic periods which reveal how important this site could be, but unfortunately, it is badly damaged and bulldozed. This paper states the results of the stratigraphy excavation of Tepe Vakilabad, where a total of 6 C-14 radiocarbon charcoal samples were collected from the only trench of this mound and analyzed by the Accelerator Mass Spectrometer (AMS) method in the laboratory of university of Lyon, France. Since the chronology of south-eastern Iran is based on the old and not very precise results of Tepe Yahya and Tal-Iblis excavations, it needs the revision. The main objective of this study was to go through the chronology table of south-eastern Iran and discuss it critically with the aid of Vakilabad and the other recent excavations results of the region, such as Tepe Dehno Shahdad. According to a comparative analysis based on the ceramics of this excavated settlement site, it could be concluded that Vakilabad belongs to Yahya V culture, and based on the absolute dating results (mostly ceramics), this site dates back to the early fifth millennium BC to the mid-fifth millennium BC. Finally, the Chalcolithic cultures of the southern Iran will be discussed in a broader context of Near East. It is obvious that the reappraisal of the chronology of this vast cultural region needs further studies, where the present paper may be able to collaborate in these researches.

The first manuscript which has been identified in the technology of making luster glaze (enamel) is the book Arayes al-Javaher. This book was compiled by Abulqasim Abdullah Kashani in 700 AH and was very effective in making the luster glaze at that time, and introduced for the first time to the world in 1313 AD. The book Javaher Name-ye- Nezami was then introduced as the oldest and most detailed historical written document on the luster glaze, where more than 26 luster formulas have been included in the book. This valuable book was compiled in 592 AH by Mohammad ibn Abi al-Barakat Neyshabouri. Previously, it was believed that Javaher Name-ye- Nezami is the oldest written document on the luster enamel. But, the emergence of book of Jaber ibn Hayan, called al-Durra al-Meknuna in recent years, by Ahmad Yusof Alhasan, revealed correctly how the father of chemistry, Jaber, deals with luster enamel formulas. He was undoubtedly the source of chemical knowledge for other scholars in later centuries. It is very important that the emergence of glass in the second century was coincided with the emergence of the painted luster glass. At the moment, the manuscript al-Durra al-Meknuna was the oldest written document on golden-colored paintings (luster enamel), where it had widespread formulas in this field. This book also contains more formulas about the luster enamels than other historical books and can be important in terms of the origin and nature of the luster -plated technique. The treatise can be divided into four main themes. The first is on the manufacture of coloured glass. The second is on lustre painting of glass and the third is on the colouring of gemstones with descriptions of two furnaces for this purpose. The last one is concerned with the treatment of pearls and gives recipes for glues and other related materials. On the other hand, the treatise contains 118 recipes for talawih (lustre painting of glass), in addition to nine recipes inserted by the editor, al-Marrakishi. However, other books have limited number of formulas, for instance, Arayes Aljvaher and Javaher Name-ye- Nezami have two and thirty formulas, respectively. In a typical process described in the book, metallic ingredients, mainly burnt silver, burnt copper or copper compounds, iron and its compounds and cobalt blue, plus other materials such as cinnabar, magnesia, realgar, orpiment, sulphur, and vitriol, are pulverised individually in vinegar or citron juice and mixed together. Glass articles such as cups are painted and decorated by the colouring mixture and are then introduced into the smoke chamber in the oven. When the cups become black, they are withdrawn and allowed to cool. Then, they are washed until the colour appears, while by introducing them again into the fire, the colour intensifies and changes. Sometimes they are introduced into the fire once again and the colour becomes brighter. The furnace designed in the book is a type of traditional wood burning stoves, where it has four shafts and a fireplace chamber. Inside it, there is a relatively large chamber for the arrangement of ceramic products. In the upper part, there is a circular door that houses the entrance and exit of the furnace to arrange the products. This kind of furnace has been widely used in most regions of Iran. In relation to the term “Zarrin fam,” various items have been mentioned in the literature such as glaze, enamel, ink, talawih, luster, gold glaze, felez fam (metal fam), but in this research, the term “enamel” has been used. The book “al Durra al-Meknuna” has several formulas, so it is recommended that these formulas to be tested on glass and glaze in the future.