Journal of Research on Archaeometry
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Showing 8 results for B. Kasiri

Masoud B. Kasiri, Hamidreza Ghorbani, Yaser Nazarieh,
year 1, Issue 1 (Semi-Annual 2015)
Abstract

Context of the archaeological findings is an important part of these artifacts and many useful information, regarding the provenance, application and dating of findings must be determined considering the characteristic of corresponding context. In some cases, the context of an historical objects is missing and hence, the accuracy of the information regarding the historical object is unsatisfactory. However, some types of laboratory experiments are able to provide the required information regarding the archaeological context of the object. In this study, it was tried to find the context of five gray Iron Age pottery pieces belong to the Museum of Ancient Iran. In order to identify and measure the elements in sediments and body of the samples, inductively coupled plasma-optical emission spectroscopy (ICP-OES) technique was used. Also, to identify the anions present in sediments on the samples, ion chromatography (IC) technique was employed. The results showed that, the sample MB-1 and MB-2, on the basis of elements present, have the same context, where the specifications are very close to the cemetery. Also, based on the high concentrations of calcium carbonate deposits in the chemical composition of MB-3, this sample could be related to the kitchen or floor of a residential area. Regarding the samples termed MB-4 and MB-5, as the results of elemental analysis showed the presence of some elements such as potassium, magnesium, iron, and titanium and, a positive correlation of these elements with each other, as well as a negative correlation between potassium and magnesium with Si, the context ought to be associated with fire, such as oven and grill found in the kitchen. Results of polarized light microscopy (PM) also showed a close correlation and structural similarity based on the type of tempering with gray earthenware tempering, traditionally used during the Iron Age, which are clay minerals having relatively smooth and homogeneous texture in all the samples.


Masoud B. Kasiri, Bahareh Younesi, Afsaneh Yajam,
year 2, Issue 1 (Semi-Annual 2016)
Abstract

Historical papers with all museum and aesthetic value have considerable cultural and scientific importance which represents how societies were during history improved. Studying historical papers is a way to discover the changes of human’s life in different cases such as economics, culture and politics. Between existing manuscripts prescriptions there are some, which are left unseen unfortunately due to lack of recognition of their writing date. So to understand their originality, we require technical and structural analyses. Quantitative and qualitative methods of analysis and identification of organic paper are able to recognize their structure and thus the probable time of the paper making process or use it as a cultural work. Today, using scientifically exact methods like radiocarbon dating of organic material such as dating paper results well. Unfortunately, it is impossible to use this method in our country because of high cost and lack of access for most of experts. In this research we seek to know the most used materials in a specific era and to make possible the indirect dating by studying and recognizing fibers and sizing in historical papers. We have used microscopic observations, color reagents and Fourier Transform Infrared Spectroscopy (FT-IR) methods. Results showed that linen, and hemp fibers have a high level of application in studied dated manuscripts and there is conformity in these results with results of studied undated ones.


Zeinab Nourzehi, Bahram Ajorloo, Masoud B. Kasiri, Ghader Ebrahimi,
year 2, Issue 2 (Semi-Annual 2017)
Abstract

In the Bronze Age Archaeology of Northwestern Iran (plateau), the advent of various types of handmade gray-black ceramics shows the arrival of the so-called Kura-Araxian culture. The Urmia Ware, dating to the Late Bronze Age, on the other hand, represents the revival of the buff painted pottery tradition, following the decline of the Early Bronze Kura-Araxian culture. The present work attempted to examine the matrixes of samples of sherds in the Early Bronze gray-black pottery of Kura-Araxes, and a further samples of sherds in the Late Bronze buff-painted pottery of Urmian Ware, all collected during the surface surveys of Kul Tepe, Ajabshir County, through the petrographic technique and observing thin-sections by polarizing microscope, as well as XRD and FT-IR analysis. The main objective was to study the similarities in the structure of the Early Bronze (Kura-Araxian) and Late Bronze (Urmian Ware) ceramics. The primary focus was on examining the possibility of local production of these ceramics through the analysis of the prepared thin-sections and ascertaining their technology, structure and composition, as well as gathering data on such fields as compositions and resources of raw material. Since Kul Tepe contains both Early Bronze and Late Bronze deposits, it offers a good opportunity for studying Archaeometrically the problem of discontinuity in technological pottery traditions, and the fact that whether the Urmian Ware tradition represented a local or an imported phenomenon. Results of the polarization microscopy, as well as the XRD and FT-IR analyses and their comparison to the available regional petrographic indices, showed that the clay used in both samples was procured from a single source, and the Early Bronze Age sherds and the Late Bronze Age painted sherds were then both manufactured locally.


Umm Al-Banin Rastineh, Masoud B. Kasiri, Bahram Ajorloo, Qader Ebrahimi,
year 3, Issue 1 (Semi-Annual 2017)
Abstract

Although the pottery is found in a massive amount in archaeological discoveries, these materials are the most important materials for different orientations in studies on the ancient people. One aspects of the study on ancient potteries, is the investigation about the painting and different colorants used for decorating potteries in variety patterns with different colors. This study aims to explore the ancient people knowledge and their experiments on creation of color by making up dying materials that could be found close to their dwells. The present work represented an attempt to discern experimentally the base and chemical composition of colorants used as decorative elements on ancient ceramics. Thus, five pieces of late Bronze painted pottery of the eastern Lake Urmia Basin (from the archaeological site of Kul Tepe of Ajabshir) were singled out. First, to determine whether the paint came from organic or inorganic sources and also to identify the existing anions and cations the Fourier-Transform Infrared Spectroscopy (FT-IR) technique was employed. The results demonstrated that the used coloring material has a mineral origin, where the sharp and strong peak at 465 cm-1 of the spectrums confirmed that the nature of coloring agents consists of iron oxides. Next, for elemental analysis and studying the chemical structure and composition of the colorants Scanning Electron Microscope-Energy Dispersive X-Ray analysis (SEM-EDX) was used. SEM-EDX analysis result demonstrated the presence of iron and manganese (Mn) content alongside other component elements of the ceramic bodies including SiO2, MgO, Al2O3, and K2O, where the results tallied with the FT-IR spectrums. On the basis of elemental analysis results, it could be said that iron oxides are the main components of coloring agents, where they could produce a variety of colors, ranging from red to dark brown. Moreover, the presence of manganese make the paintings darker, and consequently, the brighter nature of paintings of sample no. 3 of Kul Tepe and sample no. 1 of Haftvan could be the consequence of the miserable amount of this element (1.77 and 0.49%, respectively). Finally, in order to confirm and complete the study, the specimens were subjected to X-Ray Diffraction analysis (XRD). This experiment also showed that the pigments used in ornamenting the sherds were mineral and comprised of Agite mineral (Ca(Fe, Mg)Si2O6), as the coloring mineral, alongside other minerals including sodic and calcite feldspars. The results obtained are in good agreements with the geology of the region, where the feldspars exist as the main minerals of both sites. Therefore experimental analysis on the pigments structure that used in the painting of Kul Tepe Urmia ware decorations in different ways and various laboratory equipments demonstrated that the pigments used in the pottery decorations have mineral source and presented various iron compounds in the paint of decorations. As result of this study, the presence of iron compounds in the soil of the Kul Tepe region, it could be said the ancient people did use the natural sources of colorants for decoration of their potteries. Moreover, the techniques and materials used for decoration of the potteries were the same at both side of the Lake Urmia.

Leila Zarei, Masoud B. Kasiri, Mohsen Mohammadi Achachlouei, Vali Javadiazar Khiavi,
year 4, Issue 1 (Semi-Annual 2018)
Abstract

Frist Quran manuscripts remained from early centuries of Islam, have been written on skin in Quran script, and are considered as the most important works of that times. Due to the very small amount of organic matter left over the past years, the study of these works has been very limited, so the information about these works is based only on library studies, including the information contained in the old books and comparative-historical studies. One of these works is a folio of a Quran manuscript with the size of 14.5 × 9.5 cm (Property no.: 1315) which is preserved in the Quran and Redaction Museum of Tabriz. According to the materials contained in the birth certificate, this manuscript has been transferred from Golestan Palace of Tehran to this museum during the past years. Experts have identified the material and information on this skin according to the type of textbook and eventually, its adaptation to similar works. Despite its historical and cultural values, it has not been yet investigated scientifically, neither from historical nor artistic point of view. Structural study not only can be useful in assessing the authenticity of the manuscript, but also provides a detailed account of the treatment of skin in the early stages of Islamic era. It should be noted that the results of the processing method can be cited if the authenticity of the manuscript could be proved. During this research, the processing technique and constituent elements, including bedding, type of bedding, and black and red inks on it were identified and studied. The objectives of this study include examining the authenticity of the work and, in the case of authenticity, obtaining documented results in the basin of the method of dermatology in the early years of Islam. Due to the historical, cultural and religious importance and, ultimately, the sampling constraints, non-destructive methods that require less sample were used. The strategies of this research are based on ancient metamorphic and laboratory studies, including spot tests as well as instrumental techniques. In this research, this artifact has been studied using UV photography to evaluate the authenticity, FTIR investigation to recognize the support material and make distinguish between the paper and skin, electron microscopy studies to identify the type of the animal whose skin has been used, SEM imaging to explore the morphology of cross section of the skin sample, and finally, SEM-EDX analysis to study the ink which has been used to write the manuscript. The spectra of the Fourier transform infrared spectrometry indicate the proteinaceous structure of the artwork, so the support of this manuscript is of skin and not paper, thus it can be called “skin” or “parchment”. The results obtained indicate that the support material of this folio is the skin of a type of sheep. The results of the analysis of the images obtained from the SEM are such that in some places there are microcircuits and gaps in the surface of the fiber that can be caused by the pressures introduced in the production process as well as by the effects of different factors over the time (such as atmospheric and environmental factors). It is worth noting, however, that these cracks and cracks do not have a serious effect on appearance, and the skin just has somewhat lost its softness. Regarding the dark ink, the result is not certain due to the presence of too many elements, however, according to the presence of copper, Motavvas (peacock) ink is suggested. Regarding the red ink, cinnabar is suggested as mercury and sulfur elements were identified. Authenticity investigation confirms that there is no evidence of erased or added line in this folio and it can be concluded that there is no evidence of forgery in the text and signature.

Akbar Abedi, Bahram Vosough, Mehdi Razani, Masoud B. Kasiri, Daniel Steiniger, Ghader Ebrahimi,
year 5, Issue 1 (Semi-Annual 2019)
Abstract

Obsidian is a dark glass formed by very rapid solidification of volcanic lava, but in the archaeological view, this volcanic glass is an important source for prehistoric tool-making and artifacts such as arrowhead, point, flake, blade, hand axes, micro-blades and etc. Therefore, obsidian artifacts are frequently used material in prehistory and found widely in archaeological sites around the world. The provenance study of obsidian has been an issue of intense research and debate between archeaometrist and geologists. Hence, different provenance studies carried out in Anatolia and Caucasus since 1960s up to 2015, but the obsidian research in Iran is in very early stage and consider as terra incognita. According to the occurrence of lithic obsidian artifacts in most of the prehistoric archaeological sites in north-west of Iran have been recovered during last decades, various questions have been rise on the subject of the provenance of these materials. New studies on prehistoric obsidian artifacts have been done by other scholar specially Iranians during the recent years, where the main part of these studies focus on the characterization and classification of the obsidian artifacts by chemical analysis, in order to find an evidence of sourcing and provenance. More recent research showed that some obsidian tools might have come from unknown sources located in Iran (perhaps Sahand and Sabalan Mountain). This paper will try to discuss the new obsidian mine in north-west Iran in western Asia. After a brief introduction of obsidian studies in north-west Iran, the paper addresses preliminary report of recent researches that took place concerning 10 local obsidian mine samples from Tajaraq of Miyaneh and Ghizilja of Bostababad, around of Bozghoosh Mountain in the skirt of Sahand volcano. This study was realized by portable X-ray fluorescence (pXRF), as a non-distractive technique for elemental analysis, to differentiate between local obsidian mine. From 10 mine samples, 8 samples from Tajaraq of Miyaneh and 2 samples of Ghizilja of Bostanabad were selected and analyzed. This mine samples could be consider as the first obsidian source specimens in association with prehistoric lithic artifacts of north-west Iran and give the chance for detail and comparative studies of these sources with prehistoric site artifacts for provenance studies, as local or imported materials to this part of Iran. The research has been carried out with a focus on locating the origins and resources of obsidian procurement in the northwest of Iran, in order to rethink and reconstruct the regional and supra-regional trade and exchange networks in future. The project clearly identified the three groups of geochemically different obsidians named Tajaraq A, Tajaraq B, and Ghizilja. Due to the fact that Tajaraq obsidian is of a higher quality than the Ghizilja ones, it seems likely that the samples of Tajaraq obsidians have had the ability to be used for tool-making in the past, as the samples of Ghizilja, Bostanabad are too fragile and perlitic in structure. Hence, as the two groups of Tajaraq A and Tajaraq B have the ability to be used for ancient tools in all probability, they can be introduced as candidates for obsidian mining in prehistoric times in the northwest of Iran. In fact, the proposed hypothesis is still at a very early stage and future scientific studies and field research have to be followed. Comparing the new results with prehistoric sites in the cultural areas of Miyaneh and Bostanabad, it becomes obvious that the Tajaraq B obsidian overlaps in some trace elements with published data Anatolian sources. If this overlap could be found also by comparing other elements and their combination, and if it will be confirmed by other methods in future, it could lead to a complete review of all previous obsidian analysis from Iran. In other words, several samples that were up to now thought to be from Anatolia could come in reality from source B of Tajaraq. This is a serious and peculiar hypothesis, which means, at first step, more data have to be collected at the geological outcrops and especially, by analyzing the archaeological finds from well stratified context. The implications of the findings will discuss along with limitations and future research directions.

Masoud B. Kasiri, Akbar Abedi,
year 6, Issue 1 (Semi-Annual 2020)
Abstract

One of the important questions of archaeology is the study of the mobility and immigration of human groups. A common method for addressing these issues is to refer to the artifacts and archaeological findings left behind by the earlier cultures and to compare the forms, motifs, and production methods used among various ancient cultures, and hence, to explore the relationships and cultural exchanges between the societies. But, in the last three decades, the analysis of strontium isotopes in human tooth and bone samples (and even animals) has made it possible to study ancient immigration using a new method. According to the results of scientific researches, 87Sr/86Sr in each region is different due to the geological complications and the genus and stony sediments with 87Sr/86Sr of other regions. By measuring 87Sr/86Sr in bone and skeletal samples and comparing it with the average 87Sr/86Sr geological ratio in the region, the samples of the studied skeletons can be either indigenous or migratory. Since the people of the Piranshahr area in Iran have still traffic to the cities of Erbil and Sulaimaniyah in Iraq, and according to the studies, most villagers from Silveh village migrated to this region during the past century from the Iraqi Kurdistan, the immigration study of skeletons found in Tepe Silveh archaeological site could be interesting. The purpose of this study was to use the analysis of stable isotopes of strontium of the teeth and bone samples of skeletons obtained from the archaeological site of Tepe Silveh, Piranshahr, in order to determine their native or migratory nature. Tepe Silveh or as villager named “Tepe Sheikh Esmail Silveh” (N: 36° 48' 099'' – E: 45° 05' 937'' – altitude: 1567 m) is located exactly 100 m north of the Silveh village. Tepe Silveh is located in the center of intermountain river valley on the northern margin of the village, which has already been demolished and abandoned. As explained above, the reason for the destruction of the village was the sinking in the basin of the Silveh Dam. Seven Excavation trenches in Tepe Silveh have revealed, important materials from Early Chalcolithic Dalma (5000 BC) culture, Late Chalcolithic, Early Bronze Age culture of Hasan Ali or Nineveh V (3500- 2700 BC), Iron Age and Parthian periods. After a gap, Tepe Silveh have re-settled during Millde Islamic Periods (Seljuk era) and continued up to the late Islamic Period. According to the important location of Tepe Silveh and different occupation of the site deformation from Early Chalcolithic Dalma period to Islamic era, it should be suggested as a particularly important case study of migration, because it has been active and dynamic during different periods. Proximity of the site to the Iran, Iraq and Turkey adds to the importance of this study. To achieve this, the 87Sr/86Sr of the samples was measured. By comparing the ratio of strontium isotopes, it was possible to determine whether the samples were indigenous or migratory. The results obtained showed the different proportions in the analysis of strontium isotope, so that all samples could be considered non-native. Of course, this comment is only expressed on the basis of these five skeletons, and more specimens and analysis are needed to comment on the archaeological site of Piranshahr.

Mehdi Razani, Fateme Sehati, Masoud B. Kasiri,
year 7, Issue 1 (Semi-Annual 2021)
Abstract

Understanding and investigation of the principles, fundamentals, and the actions during the last century; following the emergence of the concept of “archaeometry” or “archaeological science”, that have encompassed the areas of cultural heritage, has have become a must for understanding the nature of scientific trends in archaeometry. Therefore, it is important to clarify the main definitions as the most important fundamental principles in conceptualization to create a common language. The purpose of this study was to investigate the origins of archaeometry by studying the approaches, areas, and boundaries of the related studies, to achieve the principles and basis of this scientific discipline. In Europe, archaeometric activities have been developed over the last century, with a focus on the topics and issues raised in the form of various interdisciplinary research approaches, and today, much of the research in this field of cultural heritage science is being conducted in an interdisciplinary approach, due to the variety of topics. According to a historical study of this interdisciplinary area of science, it can be said that archaeometry in the West has an archaeological origin and is related to the natural sciences. But in Iran, archaeometry was officially initiated under the domain of restoration of historical objects at the universities, began with the establishment of laboratories dedicated for archaeometrical studies in museums and research centers, and continued recently as an independent university discipline. Today, the most important axis of this scientific discipline includes: Characterization, Dating, Provenance, Authentication, Identification the objects application, Reconstruction of the ancient technologies, Science of conservation and restoration, Prospection & Remote sensing methods in archaeometry, Bioarchaeology, Geoarchaeology & Paleoclimatology, and Cyber-archaeology. The results of the investigations and studies realized in this research showed that due to the interdisciplinary nature of archaeometry in a discourse and research approach, it could not have a theoretical foundation. Meanwhile, understanding and adhering to the principles and foundations of the methodology of this interdisciplinary research approach in relation to the other sciences must be admitted. As if some rules and principles, such as the ethics in archaeometry, as a basic concern, have shaped the limitations and developed the archaeological methodological approach.


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